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Pitfalls encountered during quantitative determination of 3-alkyl-2-methoxypyrazines in grape must and wine using gas chromatography-mass spectrometry with stable isotope dilution analysis. Comprehensive two-dimensional gas chromatography-mass spectrometry and on-line liquid chromatography-multidimensional gas chromatography-mass spectrometry as potential loopholes.
Schmarr HG, Ganss S, Koschinski S, Fischer U, Riehle C, Kinnart J, Potouridis T, Kutyrev M. Schmarr HG, et al. Among authors: potouridis t. J Chromatogr A. 2010 Oct 22;1217(43):6769-77. doi: 10.1016/j.chroma.2010.06.049. Epub 2010 Jun 25. J Chromatogr A. 2010. PMID: 20637469
Analysis of carbonyl compounds via headspace solid-phase microextraction with on-fiber derivatization and gas chromatographic-ion trap tandem mass spectrometric determination of their O-(2,3,4,5,6-pentafluorobenzyl)oxime derivatives.
Schmarr HG, Potouridis T, Ganss S, Sang W, Köpp B, Bokuz U, Fischer U. Schmarr HG, et al. Among authors: potouridis t. Anal Chim Acta. 2008 Jun 9;617(1-2):119-31. doi: 10.1016/j.aca.2008.02.002. Epub 2008 Feb 9. Anal Chim Acta. 2008. PMID: 18486647