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1-Allyl-4-hydroxy-2,2-dioxo-N-(4-methoxyphenyl)-1H-2λ6,1-benzothiazine-3-carboxamide: polymorphic transition due to grinding with the loss of the biological activity.
Acta Crystallogr B Struct Sci Cryst Eng Mater. 2022 Feb 1;78(Pt 1):70-79. doi: 10.1107/S2052520621013093. Epub 2022 Jan 25.
Acta Crystallogr B Struct Sci Cryst Eng Mater. 2022.
PMID: 35129121
Biological properties of two enantiomorphic forms of N-(2,6-dimethylphenyl)-4-hydroxy-2,2-dioxo-1H-2λ6,1-benzothiazine-3-carboxamide, a structural analogue of piroxicam.
Shishkina SV, Ukrainets IV, Vashchenko OV, Voloshchuk NI, Bondarenko PS, Petrushova LA, Sim G.
Shishkina SV, et al. Among authors: bondarenko ps.
Acta Crystallogr C Struct Chem. 2020 Jan 1;76(Pt 1):69-74. doi: 10.1107/S2053229619016450. Epub 2020 Jan 1.
Acta Crystallogr C Struct Chem. 2020.
PMID: 31919309
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Synthesis, Crystal Structure, and Biological Activity of Ethyl 4-Methyl-2,2-dioxo-1H-2λ⁶,1-benzothiazine-3-carboxylate Polymorphic Forms.
Ukrainets IV, Burian AA, Baumer VN, Shishkina SV, Sidorenko LV, Tugaibei IA, Voloshchuk NI, Bondarenko PS.
Ukrainets IV, et al. Among authors: bondarenko ps.
Sci Pharm. 2018 May 30;86(2):21. doi: 10.3390/scipharm86020021.
Sci Pharm. 2018.
PMID: 29848976
Free PMC article.
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