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Synthesis of 23-, 25-, 27-, and 29-Membered ( Z)-Selective Unsaturated and Saturated Macrocyclic Lactones from 16- and 17-Membered Macrocyclic Lactones and Bromoalcohols by Wittig Reaction, Yamaguchi Macrolactonization, and Photoinduced Decarboxylative Radical Macrolactonization.
Iwasaki T, Tajimi Y, Kameda K, Kingwell C, Wcislo W, Osaka K, Yamawaki M, Morita T, Yoshimi Y. Iwasaki T, et al. Among authors: morita t. J Org Chem. 2019 Jun 21;84(12):8019-8026. doi: 10.1021/acs.joc.9b00870. Epub 2019 Jun 11. J Org Chem. 2019. PMID: 31136179
Inter- and intramolecular addition reactions of electron-deficient alkenes with alkyl radicals, generated by SET-photochemical decarboxylation of carboxylic acids, serve as a mild and efficient method for the preparation of gamma-amino acids and macrocyclic lactones.
Yoshimi Y, Masuda M, Mizunashi T, Nishikawa K, Maeda K, Koshida N, Itou T, Morita T, Hatanaka M. Yoshimi Y, et al. Among authors: morita t. Org Lett. 2009 Oct 15;11(20):4652-5. doi: 10.1021/ol9019277. Org Lett. 2009. PMID: 19751053
3,978 results