DaSilva J - Search Results

1

Enantioselective UHPLC Screening Combined with In Silico Modeling for Streamlined Development of Ultrafast Enantiopurity Assays.

Losacco GL, Wang H, Haidar Ahmad IA, DaSilva J, Makarov AA, Mangion I, Gasparrini F, Lämmerhofer M, Armstrong DW, Regalado EL. Losacco GL, et al. Among authors: dasilva j. Anal Chem. 2022 Jan 25;94(3):1804-1812. doi: 10.1021/acs.analchem.1c04585. Epub 2021 Dec 21. Anal Chem. 2022. PMID: 34931812

2

Chaotropic Effects in Sub/Supercritical Fluid Chromatography via Ammonium Hydroxide in Water-Rich Modifiers: Enabling Separation of Peptides and Highly Polar Pharmaceuticals at the Preparative Scale.

Liu J, Makarov AA, Bennett R, Haidar Ahmad IA, DaSilva J, Reibarkh M, Mangion I, Mann BF, Regalado EL. Liu J, et al. Among authors: dasilva j. Anal Chem. 2019 Nov 5;91(21):13907-13915. doi: 10.1021/acs.analchem.9b03408. Epub 2019 Oct 8. Anal Chem. 2019. PMID: 31549812

3

Interlaboratory study of a supercritical fluid chromatography method for the determination of pharmaceutical impurities: Evaluation of multi-systems reproducibility.

Dispas A, Clarke A, Grand-Guillaume Perrenoud A, Losacco LG, Veuthey JL, Gros Q, Molineau J, Noireau A, West C, Salafia F, Zoccali M, Mondello L, Guillen A, Wang J, Zhang K, Jochems P, Schad G, Nakajima K, Horie S, Joseph J, Parr MK, Billemont P, Severino A, Schneider S, Naegele E, Kutscher D, Wikfors R, Black R, Ingvaldson L, Da Silva JO, Bennett R, Regalado EL, Hoang TPT, Touboul D, Nikolova Y, Kamenova-Nacheva M, Dimitrov V, Berger BK, Schug KA, Kerviel-Guillon S, Mauge F, Takahashi M, Izumi Y, Bamba T, Rouvière F, Heinisch S, Guillarme D, Hubert P. Dispas A, et al. J Pharm Biomed Anal. 2021 Sep 5;203:114206. doi: 10.1016/j.jpba.2021.114206. Epub 2021 Jun 12. J Pharm Biomed Anal. 2021. PMID: 34146950

4

Automated ion exchange chromatography screening combined with in silico multifactorial simulation for efficient method development and purification of biopharmaceutical targets.

Losacco GL, Hicks MB, DaSilva JO, Wang H, Potapenko M, Tsay FR, Ahmad IAH, Mangion I, Guillarme D, Regalado EL. Losacco GL, et al. Anal Bioanal Chem. 2022 May;414(12):3581-3591. doi: 10.1007/s00216-022-03982-z. Epub 2022 Apr 20. Anal Bioanal Chem. 2022. PMID: 35441858

5

Parallel chiral sub/supercritical fluid chromatography screening as a framework for accelerated purification of pharmaceutical targets.

Losacco GL, DaSilva JO, Haidar Ahmad IA, Mangion I, Berger TA, Regalado EL. Losacco GL, et al. J Chromatogr A. 2022 Jul 5;1674:463094. doi: 10.1016/j.chroma.2022.463094. Epub 2022 May 7. J Chromatogr A. 2022. PMID: 35609494

6

Deuterated Modifiers in Sub/Supercritical Fluid Chromatography for Streamlined NMR Structure Elucidation.

Losacco GL, Cohen RD, DaSilva JO, Haidar Ahmad IA, Sherer EC, Mangion I, Regalado EL. Losacco GL, et al. Anal Chem. 2022 Sep 6;94(35):12176-12184. doi: 10.1021/acs.analchem.2c02623. Epub 2022 Aug 24. Anal Chem. 2022. PMID: 36001377

7

Dual-Gradient Unified Chromatography: A New Paradigm for Versatility in Simultaneous Multicomponent Analysis.

Losacco GL, Bennett R, Ahmad IAH, Barrientos RC, DaSilva JO, Dong Y, Schuppe AW, Wang Z, Aiken S, Mangion I, Aggarwal VK, Regalado EL. Losacco GL, et al. Angew Chem Int Ed Engl. 2022 Nov 7;61(45):e202208854. doi: 10.1002/anie.202208854. Epub 2022 Oct 7. Angew Chem Int Ed Engl. 2022. PMID: 36111975

8

Synthesis of a Complex and Highly Potent PCSK9 Inhibitor.

Kuethe JT, Lee J, Thaisrivongs D, Yasuda N, Pollack SR, Leone J, DaSilva J, Biba M, Tsay FR, Regalado EL, Qi J, Li H, Poggetto GD, Cohen R. Kuethe JT, et al. Among authors: dasilva j. Org Lett. 2023 Jul 14;25(27):5001-5005. doi: 10.1021/acs.orglett.3c01635. Epub 2023 Jun 29. Org Lett. 2023. PMID: 37382389

9

Electrosynthesis of iminophosphoranes and applications in nickel catalysis.

Mdluli V, Lehnherr D, Lam YH, Chaudhry MT, Newman JA, DaSilva JO, Regalado EL. Mdluli V, et al. Among authors: dasilva jo. Chem Sci. 2024 Mar 8;15(16):5980-5992. doi: 10.1039/d3sc05357a. eCollection 2024 Apr 24. Chem Sci. 2024. PMID: 38665537 Free PMC article.

10

Preparation and evaluation of novel stationary phases for improved chromatographic purification of pneumocandin B0.

Welch CJ, DaSilva JO, Nti-Gyabaah J, Antia F, Goklen K, Boyd R. Welch CJ, et al. Among authors: dasilva jo. J Chromatogr A. 2006 Jan 6;1101(1-2):204-13. doi: 10.1016/j.chroma.2005.10.009. Epub 2005 Oct 27. J Chromatogr A. 2006. PMID: 16257000

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