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Reaction of N≡W(O(t)Bu)3 with σ3λ5-phosphoranes. The [2 + 2] cycloaddition across the W≡N triple bond results in the first representative of an inorganic four-membered metallacycle with conjugated endo- and exocyclic double bonds.
Kovalenko OO, Kinzhybalo V, Lis T, Khavryuchenko OV, Rusanov EB, Brusilovets AI. Kovalenko OO, et al. Among authors: brusilovets ai. Dalton Trans. 2012 May 7;41(17):5132-6. doi: 10.1039/c2dt12492k. Epub 2012 Mar 27. Dalton Trans. 2012. PMID: 22450557