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Synthesis of chiral azides from C-2 substituted glycals and their transformation to C3-glycoconjugates and alpha-triazolo-naphthalene polyol.
Pandey RP, Maheshwari M, Hussain N. Pandey RP, et al. Chem Commun (Camb). 2023 Aug 10;59(65):9900-9903. doi: 10.1039/d3cc02423g. Chem Commun (Camb). 2023. PMID: 37498546
A Lewis-acid-mediated highly regio- and stereoselective chiral azidation of C2-substituted glycals is reported. This strategy provides excellent, scalable, and mild reaction conditions for the stereoselective introduction of the azido group at the C3-position of various C2 …
A Lewis-acid-mediated highly regio- and stereoselective chiral azidation of C2-substituted glycals is reported. This strategy provide …
Pd-catalyzed direct functionalization of glycals with cycloalkenones: application to the synthesis of chiral phenanthrenones.
Maheshwari M, Pandey RP, Hussain N. Maheshwari M, et al. Chem Commun (Camb). 2023 Jan 12;59(5):627-630. doi: 10.1039/d2cc05255e. Chem Commun (Camb). 2023. PMID: 36533688
The direct C-H functionalization of glycals with Pd(II) and subsequent insertion of cyclic enones via beta-hydride elimination is the key to the synthesis of 2C-branched glycals. The synthetic utility of this methodology for chiral phenanthrenones has also been demonstrate …
The direct C-H functionalization of glycals with Pd(II) and subsequent insertion of cyclic enones via beta-hydride elimination is the key to …
1H NMR spectroscopic study of complexation of citalopram with beta-cyclodextrin in aqueous solution.
Mashhood Ali S, Maheshwari A, Inder Fozdar B. Mashhood Ali S, et al. Magn Reson Chem. 2007 Mar;45(3):253-6. doi: 10.1002/mrc.1958. Magn Reson Chem. 2007. PMID: 17290386
All the CT proton resonances showed splitting in the presence of beta-CD, owing to chiral discrimination by the beta-CD, between the two enantiomers. The chiral discrimination appears to be due to different modes of binding of the R- and S-CT in the complexes involv …
All the CT proton resonances showed splitting in the presence of beta-CD, owing to chiral discrimination by the beta-CD, between the …