Analytical modeling of the thermomechanical behavior of ASTM F-1586 high nitrogen austenitic stainless steel used as a biomaterial under multipass deformation

Mater Sci Eng C Mater Biol Appl. 2015 Jun:51:87-98. doi: 10.1016/j.msec.2015.02.040. Epub 2015 Feb 25.

Abstract

Precipitation-recrystallization interactions in ASTM F-1586 austenitic stainless steel were studied by means of hot torsion tests with multipass deformation under continuous cooling, simulating an industrial laminating process. Samples were deformed at 0.2 and 0.3 at a strain rate of 1.0s(-1), in a temperature range of 900 to 1200°C and interpass times varying from 5 to 80s. The tests indicate that the stress level depends on deformation temperature and the slope of the equivalent mean stress (EMS) vs. 1/T presents two distinct behaviors, with a transition at around 1100°C, the non-recrystallization temperature (Tnr). Below the Tnr, strain-induced precipitation of Z-phase (NbCrN) occurs in short interpass times (tpass<30s), inhibiting recrystallization and promoting stepwise stress build-up with strong recovery, which is responsible for increasing the Tnr. At interpass times longer than 30s, the coalescence and dissolution of precipitates promote a decrease in the Tnr and favor the formation of recrystallized grains. Based on this evidence, the physical simulation of controlled processing allows for a domain refined grain with better mechanical properties.

Keywords: Biomaterial; Precipitates; Recrystallization; Z-phase.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biocompatible Materials / chemistry*
  • Compressive Strength
  • Computer Simulation
  • Elastic Modulus
  • Hardness
  • Models, Chemical*
  • Nitrogen / chemistry*
  • Phase Transition
  • Stainless Steel / chemistry*
  • Stress, Mechanical
  • Temperature
  • Tensile Strength

Substances

  • Biocompatible Materials
  • austenitic steel
  • Stainless Steel
  • Nitrogen