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Synthesis and Trace-Level Quantification of Mutagenic and Cohort-of-Concern Ciprofloxacin Nitroso Drug Substance-Related Impurities (NDSRIs) and Other Nitroso Impurities Using UPLC-ESI-MS/MS-Method Optimization Using I-Optimal Mixture Design.
ACS Omega. 2024 Feb 15;9(8):8773-8788. doi: 10.1021/acsomega.3c05170. eCollection 2024 Feb 27.
ACS Omega. 2024.
PMID: 38434810
Free PMC article.
A sensitive ultra-performance liquid chromatography-tandem mass spectrometry method for the simultaneous quantification of assay and trace-level genotoxic tosylate analogs (methyl and ethyl) in empagliflozin and its tablet dosage forms.
Nakka S, Muchakayala SK, Manabolu Surya SB.
Nakka S, et al. Among authors: manabolu surya sb.
Biomed Chromatogr. 2024 Jan;38(1):e5755. doi: 10.1002/bmc.5755. Epub 2023 Oct 30.
Biomed Chromatogr. 2024.
PMID: 37903616
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Investigating Betrixaban Maleate drug degradation profiles, isolation and characterization of unknown degradation products by mass-triggered preparative HPLC, HRMS, and NMR.
Surukonti SR, Manabolu Surya SB, Katari NK, Yerla RR.
Surukonti SR, et al. Among authors: manabolu surya sb.
J Pharm Biomed Anal. 2023 Oct 25;235:115643. doi: 10.1016/j.jpba.2023.115643. Epub 2023 Aug 12.
J Pharm Biomed Anal. 2023.
PMID: 37633165
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A sensitive UPLC-MS/MS method for the simultaneous assay and trace level genotoxic impurities quantification of SARS-CoV-2 inhibitor-Molnupiravir in its pure and formulation dosage forms using fractional factorial design.
Nakka S, Muchakayala SK, Manabolu Surya SB.
Nakka S, et al. Among authors: manabolu surya sb.
Results Chem. 2023 Dec;6:101019. doi: 10.1016/j.rechem.2023.101019. Epub 2023 Jun 27.
Results Chem. 2023.
PMID: 37396150
Free PMC article.
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Simultaneous quantification of lidocaine and prilocaine in human plasma by LC-MS/MS and its application in a human pharmacokinetic study.
Rao Yadlapalli SS, Katari NK, Manabolu Surya SB, Karra VK, Kommineni V, Jonnalagadda SB.
Rao Yadlapalli SS, et al. Among authors: manabolu surya sb.
Pract Lab Med. 2019 Jul 30;17:e00129. doi: 10.1016/j.plabm.2019.e00129. eCollection 2019 Nov.
Pract Lab Med. 2019.
PMID: 31414038
Free PMC article.
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Determination of ospemifene in human plasma by LC-MS/MS and its application to a human pharmacokinetic study.
Yadlapalli SSR, Katari NK, Manabolu Surya SB.
Yadlapalli SSR, et al. Among authors: manabolu surya sb.
Biomed Chromatogr. 2019 Apr;33(4):e4451. doi: 10.1002/bmc.4451. Epub 2019 Jan 7.
Biomed Chromatogr. 2019.
PMID: 30536649
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Bioanalytical technique for determination of tasimelteon in human plasma by LC-MS/MS and its application to pharmacokinetic study in humans.
Yadlapalli SSR, Karra VK, Kommineni V, Katari NK, Manabolu Surya SB.
Yadlapalli SSR, et al. Among authors: manabolu surya sb.
Biomed Chromatogr. 2019 Mar;33(3):e4431. doi: 10.1002/bmc.4431. Epub 2018 Dec 12.
Biomed Chromatogr. 2019.
PMID: 30412929
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