A two-dimensional NMR method for assignment of deoxyribose proton NMR signals in d(ApGpCpT)

Biochem Biophys Res Commun. 1984 Jun 29;121(3):1021-6. doi: 10.1016/0006-291x(84)90779-4.

Abstract

The ability to label the phosphoryl oxygens of d( ApGpCpT ) and thus assign the 31P signals, combined with a 2-D 31P/1H chemical shift correlated NMR spectral technique, provides a novel means for the ready assignment of the H5' and H3' protons coupled to the phosphates.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Chemical Phenomena
  • Chemistry
  • Magnetic Resonance Spectroscopy
  • Oligodeoxyribonucleotides*
  • Oligonucleotides*
  • Protons

Substances

  • Oligodeoxyribonucleotides
  • Oligonucleotides
  • Protons
  • deoxy-(adenylyl-guanylyl-cytidylyl-thymidine)