A Cu-doped Fe2O3/g-C3N4 composite, synthesized via a straightforward hydrothermal process with controlled morphologies, represents a significant advancement in supercapacitor electrode materials. This study systematically analyzes the impact of Cu doping in Fe2O3 and its synergistic combination with g-C3N4 to understand their influence on the electrochemical performance of the resulting composite, focusing on Cu doping in Fe2O3 rather than varying Fe2O3/g-C3N4 content. The comprehensive characterization of these composites involved a suite of physicochemical techniques. X-ray diffraction (XRD) confirmed the successful synthesis of the composite, while field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM) were employed to investigate the morphological attributes of the synthesized materials. X-ray photoelectron spectroscopy (XPS) spectra confirmed the elemental composition of the composite with 6% Cu doped Fe2O3/g-C3N4. The composite electrode, which incorporated 6% Cu doped Fe2O3 with g-C3N4, exhibited exceptional cycling stability, retaining 94.22% of its capacity even after 2000 charge-discharge cycles at a current density of 5 mA cm-2. Furthermore, this Cu doped Fe2O3/g-C3N4 composite electrode demonstrated impressive electrochemical performance, boasting a specific capacitance of 244.0 F g-1 and an impressive maximum energy density of 5.31 W h kg-1 at a scan rate of 5 mV s-1. These findings highlight the substantial potential of the Cu doped Fe2O3/g-C3N4 electrode for supercapacitor applications.
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