Analysis of Deformation and Properties of Composite Melon Petals via Vibration Pretreatment-Microwave Compound Curing

Polymers (Basel). 2023 Nov 26;15(23):4541. doi: 10.3390/polym15234541.

Abstract

The transition of large-scale cryogenic propellant tanks from metal to composite materials is the main trend in the global aerospace industry. Aiming to address the challenges of achieving the manufacturing of integrated and cost-effective manufacturing of aerospace cryogenic composite tanks that cannot be realized through the conventional autoclave process, and those of existing out-of-autoclave processes that are unable to effectively suppress defects under low-pressure conditions, a vibration pretreatment was innovatively introduced into the microwave curing process of composite materials in this study. Based on a systematic analysis of the inhibitory mechanisms of vibration pretreatment on void formation and the uniform heating mechanisms of microwaves in composite materials, the experimental results showed that the compound curing process enabled the production of components with complex structural features under low-pressure conditions while achieving equivalent surface precision and comprehensive properties, including porosity, interlaminar shear strength, and cryogenic permeation resistance, as those obtained through the standard 0.6 MPa autoclave process. This holds great promise for the application of out-of-autoclave processes in the manufacturing of large-scale aerospace cryogenic composite tanks.

Keywords: cryogenic composite tank; deformation deviation; melon petal; microwave curing; permeation rate; vibration pretreatment.