A new high-pressure high-temperature deformation apparatus to study the brittle to ductile transition in rocks

Rev Sci Instrum. 2023 Apr 1;94(4):043903. doi: 10.1063/5.0135947.

Abstract

Understanding the micro-mechanisms underlying the localized-ductile transition (LDT) as well as the brittle-plastic transition (BPT) has become crucial for our wider understanding of crustal processes and seismicity. Given how difficult in situ observations of these transitions are to perform, laboratory experiments might be our only way to investigate the processes active under these conditions (high T and high P). Here, we present Triaxial AppaRatus for GEoThermal energy, a new gas-based triaxial apparatus located at EPFL in Switzerland that was specifically designed to operate under conditions where both the LDT and BPT can occur in geomaterials. We show that the machine is capable of deforming rock samples at confining pressures of up to 400 MPa, temperatures of up to 800 °C, and pore pressures (liquid or gas) of up to 300 MPa while keeping the temperature gradient along samples of 40 mm in length and 20 mm in diameter minimal (less than 30 at 700 °C). Most importantly, the maximum load is 1000 kN (stresses as high as 2.2 GPa on 24 mm samples and 3 GPa on 20 mm samples), allowing for the deformation of very competent rock samples. Moreover, during deformation, the pair of syringe pore pressure pumps allow for continuous permeability or dilatancy recording. We benchmarked our machine against existing data in the literature and show that it accurately and precisely records stress, strain, permeability, pressure, and temperature.