Application of the van der Pauw method for electrical conductivity measurements at high temperatures using an insulating compressing ring

Michael S Bowen; David P Cann; C Rigel Woodside

doi:10.1063/5.0160938

Application of the van der Pauw method for electrical conductivity measurements at high temperatures using an insulating compressing ring

Rev Sci Instrum. 2023 Nov 1;94(11):114701. doi: 10.1063/5.0160938.

Authors

Michael S Bowen¹, David P Cann¹, C Rigel Woodside^{1

2}

Affiliations

¹ School of Mechanical, Industrial, and Manufacturing Engineering, Oregon State University, 2000 NW Monroe Ave., Corvallis, Oregon 97331, USA.
² National Energy Technology Laboratory, 1450 SW Queen Ave., Albany, Oregon 97321, USA.

PMID: 37930251
DOI: 10.1063/5.0160938

Abstract

High quality data on the high temperature electrical properties of ceramics, particularly oxides, is of great value for material selection, design, and modeling for a broad range of emerging applications. Utilizing the mismatch in the coefficient of thermal expansion between two materials, a purely mechanical method for establishing electrical contact in the van der Pauw geometry to measure the bulk resistivity of ceramic disks at high temperatures is presented. Measurements of a reference material, 20 mol. % Gd-doped cerium oxide, are presented up to 1000 °C. The viability of electrical measurements up to a maximum temperature of 1600 °C is also considered. Measurements are performed using multiple techniques and compared to literature values finding excellent agreement. The approach described in this work enables the van der Pauw method to be applied to many ceramic materials over a wide range of temperatures and environments.