Low-resistivity, high-resolution W-C electrical contacts fabricated by direct-write focused electron beam induced deposition

Open Res Eur. 2022 Aug 25:2:102. doi: 10.12688/openreseurope.15000.1. eCollection 2022.

Abstract

Background: The use of a focused ion beam to decompose a precursor gas and produce a metallic deposit is a widespread nanolithographic technique named focused ion beam induced deposition (FIBID). However, such an approach is unsuitable if the sample under study is sensitive to the somewhat aggressive exposure to the ion beam, which induces the effects of surface amorphization, local milling, and ion implantation, among others. An alternative strategy is that of focused electron beam induced deposition (FEBID), which makes use of a focused electron beam instead, and in general yields deposits with much lower metallic content than their FIBID counterparts. Methods: In this work, we optimize the deposition of tungsten-carbon (W-C) nanowires by FEBID to be used as electrical contacts by assessing the impact of the deposition parameters during growth, evaluating their chemical composition, and investigating their electrical response. Results: Under the optimized irradiation conditions, the samples exhibit a metallic content high enough for them to be utilized for this purpose, showing a room-temperature resistivity of 550 μΩ cm and maintaining their conducting properties down to 2 K. The lateral resolution of such FEBID W-C metallic nanowires is 45 nm. Conclusions: The presented optimized procedure may prove a valuable tool for the fabrication of contacts on samples where the FIBID approach is not advised.

Keywords: electrical contacts; focused electron beam induced deposition; nanofabrication; superconductivity; transmission electron microscopy.

Grants and funding

This research was financially supported by the European Union’s Horizon 2020 research and innovation programme under the grant agreement No [892427](Focused Ion Beam fabrication of superconducting scanning Probes [FIBsuperProbes])., the grant PID2020-112914RB-I00 funded by MCIN/AEI/10.13039/501100011033 (recipient: J.M. De Teresa), from CSIC through projects PIE202060E187 (recipient: J.M. De Teresa) and Research Platform PTI-001 (recipient: J. García-Ripoll), and by Gobierno de Aragón through the grant E13\_20R (with European Social Funds (Construyendo Europa desde Aragón) (recipient: J.M. De Teresa).