An automated algorithm for the determination of oil absorption strategy of magnetic nanoparticles from SEM images

Dhiepthie S M; Wilfred Franklin S

doi:10.1016/j.micron.2023.103505

An automated algorithm for the determination of oil absorption strategy of magnetic nanoparticles from SEM images

Micron. 2023 Sep:172:103505. doi: 10.1016/j.micron.2023.103505. Epub 2023 Jun 29.

Authors

Dhiepthie S M¹, Wilfred Franklin S²

Affiliations

¹ Department of Electronics and Communication Engineering, CSI Institute of Technology (Affiliated to Anna University,Tamil Nadu, India), Thovalai, Nagercoil, 629302, Tamil Nadu, India. Electronic address: dhiepthie93@gmail.com.
² Department of Electronics and Communication Engineering, CSI Institute of Technology (Affiliated to Anna University,Tamil Nadu, India), Thovalai, Nagercoil, 629302, Tamil Nadu, India.

PMID: 37442026
DOI: 10.1016/j.micron.2023.103505

Abstract

In recent years, the magnetic iron oxide nanoparticles (MNPs) are employed as efficient absorbents for oil removal from water. In this research, the particle size (diameter) obtained from Scanning Electron Microscopy (SEM) images of MNPs, before and after oil-absorption, are utilized to determine the oil-absorption capacity. However, the manual evaluation of the particle size and particle size distribution (PSD) are highly time-consuming and needs expertised people for accurate analysis. Hence, an image processing algorithm is employed for the determination of particle size and PSD from the Scanning Electron Microscopy (SEM) images. The key objective revolves with the preparation of the Maleic Anhydride Grafted Polypropylene anchored Magnetic Nanoparticles (MAPP-a-MNPs) to absorb crude oil from the marine water. The shape, size, and size distribution of MAPP-a-MNPs were assessed by both manual and automated analysis. For this purpose, expertise people help with the manual analysis and Threshold Adaptive-Canny Edge Detection (TA-CED) and Accumulator Updated-Circular Hough Transform (AU-CHT) method is employed for automated analysis. All the automated process were conducted in MATLAB and the measurements were taken for both before and after the oil absorption images. These measurements aid us to determine the quantity of oil absorbed by MAPP-a-MNPs. The results demonstrates excellent oil removal capacity of MAPP-a-MNPs.

Keywords: Accumulator updated-circular hough transform; Magnetic nanoparticles; Oil absorption; Scanning electron microscopy; Threshold adaptive-canny edge detection.