The Effect of Colloidal Silica and Glaze Coatings on the Adhesion of Zirconia with Various Ytrria Concentration

Eur J Prosthodont Restor Dent. 2023 Nov 30;31(4):346-357. doi: 10.1922/EJPRD_2491Villanova12.

Abstract

Purpose: This study evaluated the effect of coating traditional and translucent Y-TZP with an industrial nanometric colloidal silica or glaze before or after sintering on the adhesion of zirconia with various ytrria concentration.

Materials and methods: Specimens of Y-TZP with 3% and 5% yttria were subdivided into 5 groups (n=10), according to the coating applied and moment of application (before or after Y-TZP sintering): Control (no coating), Colloidal Silica/Sintering, Sintering/Colloidal Silica, Glaze/Sintering, Sintering/ Glaze. Lithium disilicate (LD) was used as positive control. Except for Y-TZP controls, groups were conditioned with silane before cementation with a self-adhesive resin cement. After 24 hours, the shear bond strength and failure analysis were performed. Also, analysis of specimens' surface was accomplished with SEM-EDX. Kruskal-Wallis and Dunn tests were applied to analyze differences between groups (p⟨0.05).

Results: Overall, the worst and best values of shear bond strength test were control and glaze after sintering groups. Different morphological and chemical aspects were observed in SEM-EDX analysis.

Conclusions: Coating Y-TZP with colloidal silica showed unsatisfactory results. In 3Y-TZP, the surface treatment associated with the best adhesion values was the application of glaze after zirconia sintering. However, in 5Y-TZP, glaze application can be performed before or after the zirconia sintering to optimize clinical steps.

Keywords: Ceramics; Dental Porcelain; Shear Strength; Silicon Dioxide; Surface Properties.

MeSH terms

  • Cementation
  • Ceramics / therapeutic use
  • Dental Bonding* / methods
  • Materials Testing
  • Resin Cements
  • Silicon Dioxide* / chemistry
  • Surface Properties
  • Yttrium / chemistry
  • Yttrium / therapeutic use
  • Zirconium / chemistry

Substances

  • zirconium oxide
  • Silicon Dioxide
  • Zirconium
  • Resin Cements
  • Yttrium