Crystal bending in triple-Laue X-ray interferometry. Part I. Theory

J Appl Crystallogr. 2023 May 12;56(Pt 3):707-715. doi: 10.1107/S1600576723002844. eCollection 2023 Jun 1.

Abstract

The measured value of the (220) lattice-plane spacing of silicon 28 using scanning X-ray interferometry is essential to realize the kilogram by counting 28Si atoms. An assumption made is that the measured lattice spacing is the bulk value of an unstrained crystal forming the analyser of the interferometer. However, analytical and numerical studies of the X-ray propagation in bent crystals suggest that the measured lattice spacing might refer to the analyser surface. To confirm the result of these studies and to support experimental investigations of the matter by phase-contrast topography, a comprehensive analytical model is given of the operation of a triple-Laue interferometer having the splitting or recombining crystal bent.

Keywords: Laue diffraction; bent crystals; crystal X-ray interferometry; dynamical theory of X-ray diffraction.

Grants and funding

Funding for this research was provided by Ministero dell’Istruzione, dell’Università e della Ricerca.