Preparation and Characterization of Modified Kaolin by a Mechanochemical Method

Materials (Basel). 2023 Apr 14;16(8):3099. doi: 10.3390/ma16083099.

Abstract

A mechanochemical approach was utilized to prepare modified kaolin, and the hydrophobic modification of kaolin was realized. The study aims to investigate the changes in particle size, specific surface area, dispersion ability, and adsorption performance of kaolin. The structure of kaolin was analyzed using infrared spectroscopy, scanning electron microscopy, and X-ray diffraction, and the alterations to the kaolin microstructure were thoroughly researched and discussed. The results demonstrated that this modification method can effectively improve the dispersion and adsorption capacities of kaolin. Mechanochemical modification can increase the specific surface area of kaolin particles, reduce their particle size, and improve their agglomeration behavior. The layered structure of the kaolin was partially destroyed, the degree of order was debased, and the activity of its particles was enhanced. Furthermore, organic compounds were adsorbed on the surface of the particles. The appearance of new infrared peaks in the modified kaolin's infrared spectrum suggested that the kaolin has undergone a chemical modification process, introducing new functional groups.

Keywords: KH-570; characterization; kaolin; mechanochemical method.

Grants and funding

This work was supported by the Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD).