Optimization of Vibration Pretreatment Microwave Curing in Composite Laminate Molding Process

Polymers (Basel). 2023 Jan 6;15(2):296. doi: 10.3390/polym15020296.

Abstract

Vibration pretreatment microwave curing is a high-quality and efficient composite out-of-autoclave molding process. Focusing on interlaminar shear strength, the effects of pretreatment temperature, pretreatment time and vibration acceleration on the molding performance of composite components were analyzed sequentially using the orthogonal test design method; a scanning electron microscope (SEM) and optical digital microscope (ODM) were used to analyze the void content and fiber-resin bonding state of the specimens under different curing and molding processes. The results show that the influence order of the different vibration process parameters on the molding quality of the components was: vibration acceleration > pretreatment temperature > pretreatment time. Within the parameters analyzed in this study, the optimal vibration pretreatment process parameters were: pretreatment temperature of 90 °C, pretreatment time of 30 min, and vibration acceleration of 10 g. Using these parameters, the interlaminar shear strength of the component was 82.12 MPa and the void content was 0.37%. Compared with the microwave curing process, the void content decreased by 71.8%, and the interlaminar shear strength increased by 31.6%. The microscopic morphology and mechanical properties basically reached the same level as the standard autoclave process, which achieved a high-quality out-of-autoclave curing and molding manufacturing of aerospace composite components.

Keywords: components; mechanical property; microwave curing; orthogonal experiment; out-of-autoclave; vibration pretreatment; voids.