Reconstruction algorithms for grain mapping by laboratory X-ray diffraction contrast tomography

J Appl Crystallogr. 2022 Dec 1;55(Pt 6):1652-1663. doi: 10.1107/S1600576722010214.

Abstract

X-ray-based non-destructive 3D grain mapping techniques are well established at synchrotron facilities. To facilitate everyday access to grain mapping instruments, laboratory diffraction contrast tomography (LabDCT), using a laboratory-based conical polychromatic X-ray beam, has been developed and commercialized. Yet the currently available LabDCT grain reconstruction methods are either ill-suited for handling a large number of grains or require a commercial licence bound to a specific instrument. To promote the availability of LabDCT, grain reconstruction methods have been developed with multiple reconstruction algorithms based on both forward and back calculations. The different algorithms are presented in detail and their efficient implementation using parallel computing is described. The performance of different reconstruction methods is assessed on synthetic data. The code to implement all the described algorithms has been made publicly accessible with the intention of fostering the development of grain mapping techniques on widely available laboratory instruments.

Keywords: 3D imaging; back calculations; diffraction contrast tomography; forward calculations; grain mapping; reconstruction algorithms.

Grants and funding

This work is part of the project Advanced Laboratory X-ray Microtomography funded by the Agence Nationale de la Recherche (grant No. ANR-18-CE42-0005).