The hybrid coating of curcumin and melamine was prepared by a simple electrochemical method. Some physical and chemical properties of the fiber were studied by several methods such as FT-IR, scanning electron microscopy and X-ray fluorescence spectroscopy. The fiber was stable at the inlet of a gas chromatograph at temperatures up to 280°C. The fiber has been used for the extraction of ethylbenzene, toluene and xylenes (ETX). Some parameters of headspace solid-phase microextraction, including extraction time, temperature and salt amount, were optimized. Under the optimized situation, the detection limits were 0.15-0.21 μg L -1 and the linear ranges were within the range of 0.5-1,000 μg L-1 (r2 ≥ 0.99). The intra-day and inter-day relative standard deviations were 10.2-13.7 and 13.0-15.6%, respectively, at a concentration level of 10 μg L-1 from each compound by applying a single fiber. The method was used to successfully analyze wastewater and pool water samples.
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