pH influences the volumetric change of calcium silicate- and epoxy resin-based root canal sealers: An ex vivo micro-CT study

Aust Endod J. 2023 Sep:49 Suppl 1:194-201. doi: 10.1111/aej.12716. Epub 2022 Nov 19.

Abstract

This study assessed the influence of pH variation on the volumetric change of EndoSequence BC Sealer compared to AH Plus Jet. Eighteen single-rooted teeth were uniformly prepared and filled with one of the sealers. After 24-h storing, samples were scanned in a micro-CT device. Then, roots were immersed in 20 ml phosphate-buffered saline (PBS) with pH of 5, 7 or 12 at 37°C for 7 and 30 days and rescanned. Statistical analysis was performed using Shapiro-Wilk's test, one-way ANOVA and Tukey's or Student's t-tests (p < 0.05). Differences between sealers were observed only at neutral pH and after 30 days of acidic pH exposure, with a higher loss of EndoSequence (p < 0.05). After 7 days, alkaline pH reduced and increased the volumetric loss of EndoSequence and AH Plus, respectively, compared to neutral pH (p < 0.05). It can be concluded that the pH directly influenced the volumetric change of both tested root canal sealers in different ways.

Keywords: X-ray microtomography; calcium silicate; endodontics; hydrogen-ion concentration; root canal filling materials.

MeSH terms

  • Calcium Compounds
  • Dental Pulp Cavity / diagnostic imaging
  • Epoxy Resins*
  • Humans
  • Hydrogen-Ion Concentration
  • Materials Testing
  • Root Canal Filling Materials*
  • Silicates
  • X-Ray Microtomography

Substances

  • epoxy resin-based root canal sealer
  • calcium silicate
  • Epoxy Resins
  • Root Canal Filling Materials
  • Calcium Compounds
  • Silicates