Microstructural and Textural Investigation of an Mg-Zn-Al-Ca Alloy after Hot Plane Strain Compression

Materials (Basel). 2022 Oct 26;15(21):7499. doi: 10.3390/ma15217499.

Abstract

The formability of magnesium alloys can be significantly improved by Ca as an alloying addition. Compared to conventional alloy sheets such as AZ31, texture modification can be found in rolled Mg-Ca sheets, which reveal a randomized orientation distribution. The hot deformation behavior of a twin-roll cast and homogenized Mg-2Zn-1Al-0.3Ca (ZAX210) alloy was characterized during hot compression at a temperature of 350 °C and strain rates of 0.1 s-1 and 10 s-1. Electron backscatter diffraction (EBSD) analysis was performed in order to describe the microstructural and texture evolution. The ZAX210 alloy exhibits a pronounced dynamic recrystallization (DRX) behavior during compression at high strain rates, while at lower strain rates DRX hardly occurred. This effect can be attributed to different DRX mechanisms that take place as a function of strain rate. At low strain rates, DRX occurred locally at the grain boundaries of the original microstructure, forming a so-called necklace structure. Increasing strain rate results in an increased fraction of recrystallized grains from 18% (0.1 s-1) to 39% (10 s-1). The microstructure revealed that twin boundaries act as nucleation sites for the DRX (TDRX). The recrystallized areas exhibit a weaker texture compared to the deformed microstructure.

Keywords: Mg-Zn-Al-Ca alloy; dynamic recrystallization; plane strain compression; texture; twinning.