(E)-2-(3,5-Di-meth-oxy-benzyl-idene)indan-1-one

IUCrdata. 2020 Jun 12;5(Pt 6):x200759. doi: 10.1107/S2414314620007592. eCollection 2020 Jun.

Abstract

The title chalcone, C18H16O3, was prepared by a solventless base-promoted Claisen-Schmidt condensation and, upon recrystallization from ethanol, obtained in 56% yield. The dihedral angle between the indanone ring system and the benzene ring is 2.54 (4) ° and the C atoms of the methoxy groups deviate from the benzene ring by 0.087 (1) and 0.114 (1) Å. In the crystal, π-stacking is the predominant inter-molecular force, with the mol-ecules stacking into columns running parallel to the b axis of the unit cell.

Keywords: chalcone; crystal structure; green synthesis; indanone.

Grants and funding

Funding for this research was provided by: GGC STEC 4500 Research Fund.