Porous intermetallic Ni2XAl (X = Ti or Zr) nanoparticles with small crystallite sizes (24-34 nm) and high Brunauer-Emmett-Teller (BET) surface areas (10-71 m2 g-1) were prepared from oxide precursors by a chemical route. CaH2 acted as a template to form the porous morphologies and assisted the reduction.
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