Synthesis Metakaolin-Based Geopolymer Incorporated with SiC Sludge Using Design of Experiment Method

Polymers (Basel). 2022 Aug 19;14(16):3395. doi: 10.3390/polym14163395.

Abstract

This study uses metakaolin, sodium hydroxide, sodium metasilicate, and water content as the reaction variables in the application of the design of experiment (DOE) method. At the same time, the various component factors and their interactions were analyzed to understand how these factors affect the mechanical properties of a metakaolin-based geopolymer incorporated with SiC sludge (SCSGPs). The results of the statistical analysis showed that the compressive strength of SCSGPs was affected by the Na/Si molar ratio (NSR) (p-level = 0.000 <0.05), the Na/Al molar ratio (NAR) (p-level= 0.000 <0.05), and the interaction between the dissolution rate of Si (DRA). Within the design scope of this study, the maximum compressive strength of SCSGPs and the coefficients of the NSR, the NAR, and the DRA of SCSGPs was evaluated. The multiple regression analysis and the tested coefficient of r2 were also studied. The multiple regression analysis models provide an effective reference for the application of SCSGPs.

Keywords: SiC sludge; design of experiment; factor parameter; interaction; multivariate regression model.

Grants and funding

This research was funded by the Ministry of Science and Technology, Taiwan, grant number MOST-109-2221-E-197-012-MY3.