Monitoring and Visualization of Crystallization Processes Using Electrical Resistance Tomography: CaCO3 and Sucrose Crystallization Case Studies

Sensors (Basel). 2022 Jun 11;22(12):4431. doi: 10.3390/s22124431.

Abstract

In the current research work, electrical resistance tomography (ERT) was employed for monitoring and visualization of crystallization processes. A first-of-its-kind MATLAB-based interactive GUI application "ERT-Vis" is presented. Two case studies involving varied crystallization methods were undertaken. The experiments were designed and performed involving calcium carbonate reactive (precipitative) crystallization for the high conductivity solution-solute media, and the cooling crystallization of sucrose representing the lower conductivity solution-solute combination. The software successfully provided key insights regarding the process in both crystallization systems. It could detect and separate the solid concentration distributions in the low as well as high conductivity solutions using the visual analytics tools provided. The performance and utility of the software were studied using a software evaluation case study involving domain experts. Participant feedback indicated that ERT-Vis software helps by reconstructing images instantaneously, interactively visualizing, and evaluating the output of the crystallization process monitoring data.

Keywords: crystallization process monitoring; electrical resistance tomography; process operation; visualization.

MeSH terms

  • Crystallization
  • Electric Impedance
  • Humans
  • Solutions
  • Sucrose* / chemistry
  • Tomography*

Substances

  • Solutions
  • Sucrose