A split-Chevron-Notched-Beam sandwich specimen for fracture toughness testing of bonded interfaces

J Mech Behav Biomed Mater. 2022 Jul:131:105236. doi: 10.1016/j.jmbbm.2022.105236. Epub 2022 Apr 12.

Abstract

The realization that the use of strength tests as a means to probe the bonding performance of adhesive systems to dental restorative materials suffers from inherent drawbacks has shifted efforts towards devising viable and valid fracture toughness test for that purpose. Here we introduce a new procedure to produce split-Chevron-Notched-Beam specimens that need not undergo sawing or notching after bonding, thus sparing the interface from pre-stresses. We evaluate the formal geometric factor considering the influence of the use of different materials having different elastic properties, and show that the results obtained fall within reasonable ranges measured by other established compliance calibrated methods. We demonstrate the application of this new approach for dentin-luting composite and zirconia-luting composite interfaces for different adhesive systems and pre-treatment procedures in order to probe the sensitivity of the method to different bond qualities.

Keywords: Adhesion; Bonding; Chevron-notched-beam; Dentin; Fracture toughness; Zirconia.

MeSH terms

  • Adhesives
  • Composite Resins / chemistry
  • Dental Bonding*
  • Dental Stress Analysis
  • Dentin
  • Dentin-Bonding Agents* / chemistry
  • Materials Testing / methods
  • Resin Cements / chemistry
  • Stress, Mechanical
  • Surface Properties

Substances

  • Adhesives
  • Composite Resins
  • Dentin-Bonding Agents
  • Resin Cements