Direct digestion of human scalp hair on the substrate used for total reflection X-ray fluorescence analysis

Anal Sci. 2022 May;38(5):821-824. doi: 10.1007/s44211-022-00095-6. Epub 2022 Mar 28.

Abstract

It is important to determine the elemental content of scalp hair to evaluate human health and environmental contamination. Here, a new sample preparation method for total reflection X-ray fluorescence analysis was developed by directly digesting the human hair on the sample holder. A human hair sample was subjected to thermal nitric acid treatment for sample digestion and homogenization. The Zn concentration was estimated to be ~ 1.89 × 102 μg/g. We can evaluate other elements of human hair by using this method.

Keywords: Direct digestion on substrate; Human hair; Total reflection X-ray fluoresence analysis; Trace elements analysis.

MeSH terms

  • Digestion
  • Fluorescence
  • Hair / chemistry
  • Humans
  • Scalp* / chemistry
  • Trace Elements* / analysis
  • X-Rays

Substances

  • Trace Elements