To improve the adsorption performance of carbon materials, novel ZnO nanoparticle-incorporated porous carbon nanofibers (Zn@PCNFs) were prepared via an electrospinning technique. A facile one-step fabrication strategy was proposed to simultaneously complete the carbonization of a peroxided polyacrylonitrile framework, the activating treatment caused by ZnO reducing to Zn, and the pore generation caused by evaporation of reduced Zn with a low melting point. The influences of the pH, ion category, and concentration on methylene blue adsorption were investigated. The physical-chemical characterizations showed that ZnO was homogeneously distributed on the nanofibers and micropores were generated. The adsorption results revealed that an efficient adsorption was obtained within a large range of pH values through different adsorption models, which was accelerated by increasing the temperature. Therefore, the novel Zn@PCNFs are anticipated to be applied in the future as an effective dye waste adsorbent.
© 2022 The Authors. Published by American Chemical Society.