Evaluation of extremely steep residual stress gradients based on a combined approach using laboratory-scale equipment

J Appl Crystallogr. 2021 Nov 30;54(Pt 6):1793-1798. doi: 10.1107/S1600576721010335. eCollection 2021 Dec 1.

Abstract

Surface treatments characterized by rapid heating and cooling (e.g. laser hardening) can induce very steep residual stress gradients in the direct vicinity of the area being treated. These gradients cannot be characterized with sufficient accuracy by means of the classical sin2Ψ approach applying angle-dispersive X-ray diffraction. This can be mainly attributed to limitations of the material removal method. In order to resolve residual stress gradients in these regions without affecting the residual stress equilibrium, another angle-dispersive approach, i.e. the universal plot method, can be used. A novel combination of the two approaches (sin2Ψ and universal plot) is introduced in the present work. Prevailing limits with respect to profiles as a function of depth can be overcome and, thus, high-resolution surface layer characterization is enabled. The data obtained are discussed comprehensively in comparison with results elaborated by energy-dispersive X-ray diffraction measurements.

Keywords: angle-dispersive diffraction; energy-dispersive diffraction; laser surface hardening; residual stress analysis.