Bonding properties of third-generation zirconia CAD-CAM blocks for monolithic restorations to composite and resin-modified glass-ionomer cements

J Prosthodont Res. 2022 Jul 30;66(3):466-475. doi: 10.2186/jpr.JPR_D_21_00044. Epub 2021 Dec 2.

Abstract

Purpose: To compare the interfacial fracture toughness (IFT) of two MDP-based composite cements and a resin-modified glass-ionomer cement (RMGIC) with third-generation zirconia CAD-CAM restorations using two different airborne-particle abrasion (AB) pressures.

Methods: Blocks were cut into prisms (n=60), split and sintered to the desired equilateral half prisms. Half-prisms were divided into two groups for AB at 0.5 or 2.5 bar with 50 µm Al2O3 particles. Each group was then further divided into 3 subgroups, and half-prisms were bonded to their counterparts with Panavia V5 (V5), Panavia Self Adhesive Cement Plus (SA), or RMGIC Fuji Plus (n=10/group). The IFT was determined using the Notchless Triangular Prism test in a water bath at 36°C after thermocycling (10,000 cycles). Surface roughness and SEM analyses were performed for representative zirconia samples after AB, and composite cements were tested for flexural strength and wettability.

Results: SA (2.5 bar) showed a significantly higher IFT. The 3 other groups with SA and V5 showed no significant difference in their IFT values regardless of the AB pressure (1-way ANOVA). Weibull analysis of SA was higher than V5. All RMGIC samples debonded while thermocycling, and were, therefore, not included in the statistical analysis. Surface roughness increased with increasing AB pressure, and both cements showed similar flexural strength values and good wettability.

Conclusion: Contrary to RMGIC, composite cements show high performance with zirconia after AB. Increasing AB pressure enhances the micromechanical retention of composite cement. Future perspectives should include study of the effect of AB pressure on zirconia surface properties.

Keywords: Adhesive dentistry; Alumina blasting; Dental bonding; Interfacial fracture toughness; Resin cements.

MeSH terms

  • Computer-Aided Design
  • Dental Bonding*
  • Dental Cements
  • Dental Stress Analysis
  • Glass Ionomer Cements*
  • Materials Testing
  • Resin Cements
  • Surface Properties
  • Zirconium

Substances

  • Dental Cements
  • Glass Ionomer Cements
  • Resin Cements
  • Zirconium
  • zirconium oxide