WAXD, polarized ATR-FTIR and DSC data of stress-annealed poly(3-hydroxybutyrate) fibers

E Perret; K Sharma; S Tritsch; R Hufenus

doi:10.1016/j.dib.2021.107523

WAXD, polarized ATR-FTIR and DSC data of stress-annealed poly(3-hydroxybutyrate) fibers

Data Brief. 2021 Oct 27:39:107523. doi: 10.1016/j.dib.2021.107523. eCollection 2021 Dec.

Authors

E Perret^{1

2}, K Sharma^{1

3}, S Tritsch^{1

4}, R Hufenus¹

Affiliations

¹ Laboratory for Advanced Fibers, Empa, Swiss Federal Laboratories for Materials Science and Technology, Lerchenfeldstrasse 5, 9014 St. Gallen, Switzerland.
² Center for X-ray Analytics, Empa, Swiss Federal Laboratories for Materials Science and Technology, Überlandstrasse 129, 8600 Dübendorf, Switzerland.
³ KTH Royal Institute of Technology, Stockholm, 114 16 Sweden.
⁴ Hochschule Reutlingen, Alteburgstrasse 150, 72762 Reutlingen, Germany.

Abstract

This article summarizes synchrotron wide-angle x-ray diffraction (WAXD) patterns, polarized attenuated Fourier transform infrared spectroscopy (ATR-FTIR) data and differential scanning calorimetry (DSC) data of differently stress-annealed poly(3-hydroxybutyrate) (P3HB) fibers. Additionally, in-situ polarized ATR-FTIR data has been measured under tensile drawing of pre-annealed P3HB fibers under low annealing stress. Modifications to the ATR-FTIR setup and sample holders for performing measurements on P3HB fibers are explained in the experimental section. For more information see 'Reversible mesophase in stress-annealed poly(3-hydroxybutyrate) fibers: A synchrotron x-ray and polarized ATR-FTIR study' [1].

Keywords: Biodegradable; Fiber; Melt-spun; P3HB; Polarized attenuated total reflection Fourier Transform infrared spectroscopy; Stress annealing; Wide-angle x-ray diffraction; poly(3-hydroxybutyrate).