Lipid-soluble vitamins from dairy products: Extraction, purification, and analytical techniques

Emad Karrar; Isam A Mohamed Ahmed; Muhammad Faisal Manzoor; Wei Wei; Frederick Sarpong; Xingguo Wang

doi:10.1016/j.foodchem.2021.131436

Lipid-soluble vitamins from dairy products: Extraction, purification, and analytical techniques

Food Chem. 2022 Mar 30;373(Pt B):131436. doi: 10.1016/j.foodchem.2021.131436. Epub 2021 Oct 20.

Authors

Emad Karrar¹, Isam A Mohamed Ahmed², Muhammad Faisal Manzoor³, Wei Wei¹, Frederick Sarpong⁴, Xingguo Wang⁵

Affiliations

¹ National Engineering Research Center for Functional Food, Collaborative Innovation Center of Food Safety and Quality Control in Jiangsu Province, School of Food Science and Technology, Jiangnan University, Wuxi 214122, Jiangsu, People's Republic of China.
² Department of Food Science and Nutrition, College of Food and Agricultural Sciences, King Saud University, Riyadh 11451, Saudi Arabia.
³ School of Food and Biological Engineering, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, Jiangsu, People's Republic of China.
⁴ Value Addition Division, Oil Palm Research Institute, Council for Scientific and Industrial Research, Kade, Ghana.
⁵ National Engineering Research Center for Functional Food, Collaborative Innovation Center of Food Safety and Quality Control in Jiangsu Province, School of Food Science and Technology, Jiangnan University, Wuxi 214122, Jiangsu, People's Republic of China. Electronic address: xingguow@jiangnan.edu.cn.

PMID: 34740052
DOI: 10.1016/j.foodchem.2021.131436

Abstract

Milk and dairy products are considered as essential sources of lipid-soluble vitamins (LSVs) for human nutrition. Due to the lower concentrations, complexity, and instability of LSVs during extraction, their quantification remains challenging. This review focus on advances in the extraction and quantification of LSVs from different dairy products. Saponification, and liquid-liquid (LLE), solid-phase (SPE), and supercritical fluid (SFE) extraction methods, as well as dispersive liquid-liquid microextraction, are the most common techniques. Liquid chromatography-mass spectrophotometry (LC-MS) has unique advantages for LSVs determination and quantification due to its high sensitivity and specificity.

Keywords: Chromatographic analysis; Lipid-soluble vitamins; Milk; Sample preparation.

Publication types

Review

MeSH terms

Animals
Chromatography, Liquid
Humans
Lipids
Milk / chemistry
Solid Phase Extraction*
Vitamins* / analysis

Substances

Lipids
Vitamins