An Attempt to Track Two Grades of Road Bitumen from Different Plants Using Fourier Transform Infrared Spectroscopy

Materials (Basel). 2021 Oct 7;14(19):5870. doi: 10.3390/ma14195870.

Abstract

This study aimed to evaluate the possibility of using Fourier Transform Infrared (FTIR) spectroscopy to track binders produced by three different plants: plants A, B, and C. The work included the quality assessment of 80 bituminous materials graded as BND 70/100 and 100/130 according to GOST 33133 (Russian interstate standard) and chemical analyses using FTIR spectroscopy. FTIR analyses were conducted before and after short-term ageing in a Rolling Thin Film Oven Test (RTFOT). Thus, the number of binder samples was multiplied by two (2) for a final total of 160 infrared (IR) spectra. All infrared spectra were normalised to ensure the reliability of results, and the standard deviation and variance coefficient were included. The principal purpose of the present work was to track the origin and the ageing extent of the bituminous binders under study.

Keywords: Fourier Transform Infrared Spectroscopy (FTIR); ageing; road bitumen; spectrometry indices; tracking; variance coefficient.