Room temperature liquid metals are an emerging class of materials for a variety of heterogeneous catalytic reactions. In this work we explore the use of Ga based liquid metals as a sonochemical catalyst for the degradation of organic azo dyes such as methyl orange, congo red and eriochrome black T. Rapid degradation to non toxic solid carbon particles was achieved over a large dye concentration range to produce differently sized particles via both bath and probe sonication which could be repeated multiple times with the same catalyst.