Linear Friction Welding of an AZ91 Magnesium Alloy and the Effect of Ca Additions on the Weld Characteristics

Materials (Basel). 2021 Jun 7;14(11):3130. doi: 10.3390/ma14113130.

Abstract

Solid-state welding offers distinct advantages for joining reactive materials, such as magnesium (Mg) and its alloys. This study investigates the effect of linear friction welding (LFW) on the microstructure and mechanical properties of cast AZ91 (Mg-9Al-1Zn) and AZ91-2Ca alloys, which (to the best knowledge of the authors) has not been reported in the literature. Using the same set of LFW process parameters, similar alloy joints-namely, AZ91/AZ91 and AZ91-2Ca/AZ91-2Ca-were manufactured and found to exhibit integral bonding at the interface without defects, such as porosity, inclusions, and/or cracking. Microstructural examination of the AZ91/AZ91 joint revealed dissolution of the Al-rich second phase in the weld zone, while the Mn containing phases remained and were refined. In the AZ91-2Ca/AZ91-2Ca joint, the weld zone retained Ca- and Mn-rich phases, which were also refined due to the LFW process. In both joint types, extensive recrystallization occurred during LFW, as evidenced by the refinement of the grains from ~1000 µm in the base materials to roughly 2-6 µm in the weld zone. These microstructural changes in the AZ91/AZ91 and AZ91-2Ca/AZ91-2Ca joints increased the hardness in the weld zone by 32%. The use of digital image correlation for strain mapping along the sample gage length during tensile testing revealed that the local strains were about 50% lower in the weld zone relative to the AZ91 and AZ91-2Ca base materials. This points to the higher strength of the weld zone in the AZ91/AZ91 and AZ91-2Ca/AZ91-2Ca joints due to the fine grain size, second phase refinement, and strong basal texture. Final fracture during tensile loading of both joints occurred in the base materials.

Keywords: FactSage-FTlite; X-ray diffraction; aerospace; calcium; digital image correlation; linear friction welding; magnesium; strain mapping; tensile testing; texture.