Stir bar sorptive extraction and its application

J Chromatogr A. 2021 Jan 25:1637:461810. doi: 10.1016/j.chroma.2020.461810. Epub 2020 Dec 15.

Abstract

Recent progress of stir bar sorptive extraction (SBSE) in the past six years is reviewed. The preparation methods including electrodeposition, self-assembly, solvent exchange, physical magnetic adsorption and electrostatic spinning, for the coated stir bar are summarized and compared, specifically for a specific material for coatings fabrication, e.g., carbon-based materials and metal organic frameworks. The emerging materials (e.g., graphene, graphene oxide, carbon nanotubes, monolith, metal-organic frameworks and porous organic polymers) applied for coated stir bar fabrication are one of the focus of this review, along with their respective advantages in extraction process and application in trace analysis. The development and application of extraction apparatus of SBSE are also involved. Based on these information, the development status and prospects of SBSE as an efficient sample pretreatment technique in real sample analysis are discussed.

Keywords: Coating preparation method; Extraction apparatus; Sorbents; Stir bar sorptive extraction; Trace analysis.

Publication types

  • Review

MeSH terms

  • Adsorption
  • Metal-Organic Frameworks / chemistry
  • Nanotubes, Carbon / chemistry*
  • Polymers
  • Porosity
  • Reproducibility of Results
  • Solvents

Substances

  • Metal-Organic Frameworks
  • Nanotubes, Carbon
  • Polymers
  • Solvents