The effect of different aging protocols on the flexural strength and phase transformations of two monolithic zirconia ceramics

J Appl Biomater Funct Mater. 2020 Jan-Dec:18:2280800020982677. doi: 10.1177/2280800020982677.

Abstract

Introduction: The aim of the present study was to investigate how different aging protocols can affect the flexural strength and phase transformations of yttrium-stabilized zirconia ceramics (Y-TZP) for monolithic restorations.

Materials and methods: Bar-shaped specimens from two zirconia ceramics bars were divided into three groups: a. no treatment (c), b. aging in an autoclave (a), and c. thermal cycling (t). The flexural strength was determined by the 3-point bending test and statistical analysis was performed to determine significant differences (p< 0.05). Weibull statistics was used to analyze the dispersion of strength values while surface microstructural analysis was performed through X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM).

Results: Aging did not significantly affect the flexural strength but differences were recorded between the two groups, with group A presenting higher strength values and m-phase percentages.

Conclusions: The observed differences between the two ceramics could be attributed to variations in composition and processing.

Keywords: Autoclave aging; Weibull statistics; flexural strength; monolithic zirconia; thermal cycling.

MeSH terms

  • Ceramics
  • Dental Materials
  • Flexural Strength*
  • Materials Testing
  • Stress, Mechanical
  • Surface Properties
  • Yttrium
  • Zirconium*

Substances

  • Dental Materials
  • Yttrium
  • Zirconium
  • zirconium oxide