A better understanding of the behavior of asphaltenes is paramount for improving processes related to heavy crude oil, such as transport. Previous research has studied its aggregation [1], as well as its average chemical structure [2]. But, of course, this expands beyond the realm of oil, as other applications are affected by asphaltenes [3]. This work presents the collected data from electrodeposited asphaltenes. We used an H-type cell, with a capacity of 300 ml, and a bridge length of 30 cm. A constant voltage of 300 Vs (DC) was applied to steel electrodes of 3 cm × 9 cm. The generated electric field was of 1000 V/m, (E = Voltage (V)/distance (m)). The previously described assembly was modified, adding a dynamic magnetic field of 4 mT and 1% w/w of magnetic nanoparticles. Afterward, we analyzed deposits at the anode and cathode using the DSC-TGA Netzsch 449 F1 equipment. Through it, we gathered the calorimetric (DSC) and thermogravimetric (TGA) data. Moreover, the Proteus analysis software was used to generate DTGA data from the TGA values. The same procedure and analysis were repeated for asphaltenes of the same oil but obtained through precipitation with heptane. Our data may pave the road for research seeking to improve the extraction, transport and refining of heavy crudes. The reason: asphaltenes are responsible for the high viscosity of hydrocarbons. So, thermal processes are customary. Our thermogravimetric data may prove fruitful in the improvement and development of said processes.
Keywords: Asphaltene; Differential scanning calorimetry (DSC); Electrodeposition; Extra heavy oil; Nanoparticles; Thermogravimetry (TGA).
© 2020 The Author(s).