Evaluation of shear bond strength of zirconia-based monolithic CAD-CAM materials to resin cement after different surface treatments

Niger J Clin Pract. 2019 Nov;22(11):1475-1482. doi: 10.4103/njcp.njcp_157_19.

Abstract

Objective: To compare the shear bond strength of resin cement to zirconia-based monolithic CAD-CAM materials subjected to different surface treatments.

Methods: 2 brands of monolithic zirconia blocks (Vita YZ HT, Sirona inCoris TZI), yttrium-stabilized tetragonal zirconia (IPS e.max ZirCAD) and zirconia-reinforced lithium silicate ceramic (Vita Suprinity) were divided into six groups according to the surface treatment received: no treatment (control), HF acid etching, sandblasting, sandblasting + Er:YAG laser irradiation, Er:YAG laser irradiation and CoJet. Composite resin cylinders were bonded to blocks with self-adhesive resin cement (Theracem). Shear bond strength was evaluated after thermocyling. Failure modes were examined using SEM. Data was analyzed statistically by using 2-way ANOVA and post-hoc Tukey's test (P < 0,05).

Results: The bond strength was significantly affected by the surface treatment and the type of CAD-CAM blocks (P < 0,001). Surface treatment with CoJet revealed significantly higher bond strength compared to sandblasting in Y-TZP and monolithic zirconia specimens.

Conclusions: Monolithic zirconia blocks showed higher bond strength values compared to Y-TZP zirconia block in sandblasting and CoJet groups. HF acid etching is more effective than sandblasting and CoJet for Vita Suprinity.

Keywords: Bond strength; CAD-CAM; monolithic zirconia; self-adhesive resin cement; surface treatment.

MeSH terms

  • Ceramics / chemistry*
  • Composite Resins / chemistry*
  • Computer-Aided Design
  • Dental Bonding
  • Humans
  • Materials Testing / methods*
  • Microscopy, Electron, Scanning
  • Resin Cements / chemistry*
  • Shear Strength*
  • Surface Properties
  • Yttrium
  • Zirconium*

Substances

  • Composite Resins
  • Resin Cements
  • VITA Suprinity
  • Adhesive cement
  • Yttrium
  • Zirconium
  • zirconium oxide