Preparation, properties, and structural characterization of β-glucan/pullulan blend films

Int J Biol Macromol. 2019 Nov 1:140:1269-1276. doi: 10.1016/j.ijbiomac.2019.08.208. Epub 2019 Aug 27.

Abstract

This study investigates the physico-mechanical and structural properties of β-glucan (BG)/pullulan (PUL) composite edible films successfully prepared with 0-0.3 g of BG. Results demonstrated that BG addition significantly increases the elongation at break (p < 0.05), tensile strength, and water dissolution time of the resulting films. The transparency of the 0.2PUL:0.1BG film and the oxygen barrier property of the 0.15PUL:0.15BG film decreased remarkably compared with those of the plain films (0.3PUL:0BG and 0PUL:0.3BG) and other composite films (p < 0.05). FTIR indicated hydrogen bonding interactions between PUL and BG molecules, and microstructural observations showed that aggregated BG is homogeneously dispersed in the PUL continuous matrix. Among the films tested, the thermal stability of the 0.15PUL:0.15BG film was the best. A PUL:BG mixing ratio of 0.15:0.15 is thus suggested to provide the best film properties. This research offers an alternative method to improve PUL-based edible films.

Keywords: Edible film; Pullulan; Structural properties; β-Glucan.

MeSH terms

  • Calorimetry, Differential Scanning
  • Glucans / chemical synthesis*
  • Glucans / chemistry*
  • Oxygen / analysis
  • Permeability
  • Rheology
  • Solubility
  • Solutions
  • Spectroscopy, Fourier Transform Infrared
  • Steam
  • Viscosity
  • Water / chemistry
  • X-Ray Diffraction
  • beta-Glucans / chemical synthesis*
  • beta-Glucans / chemistry*

Substances

  • Glucans
  • Solutions
  • Steam
  • beta-Glucans
  • Water
  • pullulan
  • Oxygen