Optimization of Spray-Drying Process of Jerusalem artichoke Extract for Inulin Production

Molecules. 2019 Apr 29;24(9):1674. doi: 10.3390/molecules24091674.

Abstract

Jerusalem artichoke is an important natural matrix for inulin production. In this experiment, response surface methodology (RSM) was employed to optimize the spray-drying parameters in order to determine the maximal inulin yield. For this study, three independent variables (heating temperature (Tª, 110-120 °C), creep speed (V, 18-22 rpm) and pressure (P, 0.02-0.04 MPa)) were used in the experimental design. Using the Box-Behnken design, the optimal parameters obtained were: drying temperature 114.6 °C, creep speed 20.02 rpm, and pressure: 0.03 MPa. The inulin yield, water content and particle size of inulin obtained by spray-drying and freeze-drying were compared. In this regard, the spray-dried inulin consisted of a white powder having a fine particle size, and the freeze-dried inulin had a pale-yellow fluffy floc. On the other hand, the drying methods had a great influence on the appearance and internal structure of inulin powder, since the spray-dried inulin had a complete and uniform shape and size, whereas the freeze-dried inulin had a flocculated sheet structure. The analysis showed that the spray-drying led to a higher inulin yield, lower water content and better surface structure than freeze-drying.

Keywords: Jerusalem artichoke; inulin; response surface methodology; spray-drying.

MeSH terms

  • Chemistry, Pharmaceutical / methods*
  • Freeze Drying / methods
  • Helianthus / chemistry*
  • Inulin / chemistry*
  • Inulin / ultrastructure
  • Plant Extracts / chemistry*
  • Powders

Substances

  • Plant Extracts
  • Powders
  • Inulin