A study of the flexural strength and surface hardness of different materials and technologies for occlusal device fabrication

Vladimir Prpic; Ivan Slacanin; Zdravko Schauperl; Amir Catic; Niksa Dulcic; Samir Cimic

doi:10.1016/j.prosdent.2018.09.022

A study of the flexural strength and surface hardness of different materials and technologies for occlusal device fabrication

J Prosthet Dent. 2019 Jun;121(6):955-959. doi: 10.1016/j.prosdent.2018.09.022. Epub 2019 Jan 31.

Authors

Vladimir Prpic¹, Ivan Slacanin², Zdravko Schauperl³, Amir Catic⁴, Niksa Dulcic⁴, Samir Cimic⁵

Affiliations

¹ Doctoral student, School of Dental Medicine, University of Zagreb, Zagreb, Croatia.
² Postgraduate student, Faculty of Mechanical Engineering and Naval Architecture, University of Zagreb, Zagreb, Croatia.
³ Associate Professor, Department for Materials, Faculty of Mechanical Engineering and Naval Architecture, University of Zagreb, Zagreb, Croatia.
⁴ Associate Professor, Department of Prosthodontics, School of Dental Medicine, University of Zagreb, Zagreb, Croatia.
⁵ Assistant Professor, Department of Prosthodontics, School of Dental Medicine, University of Zagreb, Zagreb, Croatia. Electronic address: scimic@sfzg.hr.

PMID: 30711296
DOI: 10.1016/j.prosdent.2018.09.022

Abstract

Statement of problem: With the emergence of digital technologies, new materials have become available for occlusal devices. However, data are scarce about these different materials and technologies and their mechanical properties.

Purpose: The purpose of this in vitro study was to investigate the flexural strength and surface hardness of different materials using different technologies for occlusal device fabrication, with an emphasis on the digital technologies of computer-aided design and computer-aided manufacturing (CAD-CAM) and 3D printing.

Material and methods: A total of 140 rectangular specimens were fabricated from two 3D-printed (VarseoWax Splint and Ortho Rigid), 2 CAD-CAM-produced (Ceramill Splintec and CopraDur), and 3 conventional autopolymerizing occlusal device materials (ProBase Cold, Resilit S, and Orthocryl) according to ISO 20795-1:2013. Flexural strength and surface hardness were determined for 10 specimens of each tested material using the 3-point bend test and the Brinell method. The data were analyzed using descriptive statistics and 1-way ANOVA with Bonferroni corrections (α=.05).

Results: Surface hardness values ranged from 28.5 ±2.5 MPa to 116.2 ±1.6 MPa. During flexural testing, neither the CopraDur nor the VarseoWax Splint specimens fractured during loading within the end limits of the penetrant's possible movement. Flexural strength values for other groups ranged from 75.0 ±12.0 MPa to 104.9 ±6.2 MPa. Statistical analysis determined significant differences among the tested materials for flexural strength and surface hardness.

Conclusions: Mechanical properties among different occlusal device materials were significantly different. Acrylic resins were less flexible than polyamide and nonacrylic occlusal device materials for 3D printing but had higher and more consistent values of surface hardness. Clinicians should consider the different mechanical properties of the available materials when choosing occlusal device materials.

MeSH terms

Computer-Aided Design*
Flexural Strength*
Hardness
Materials Testing
Pliability
Stress, Mechanical
Surface Properties