Vacuum Casting and Mechanical Characterization of Nanocomposites from Epoxy and Oxidized Multi-Walled Carbon Nanotubes

Molecules. 2019 Jan 31;24(3):510. doi: 10.3390/molecules24030510.

Abstract

Sample preparation is an important step when testing the mechanical properties of materials. Especially, when carbon nanotubes (CNT) are added to epoxy resin, the increase in viscosity complicates the casting of testing specimens. We present a vacuum casting approach for different geometries in order to produce specimens from functional nanocomposites that consist of epoxy matrix and oxidized multi-walled carbon nanotubes (MWCNTs). The nanocomposites were characterized with various mechanical tests that showed improved fracture toughness, bending and tensile properties performance by addition of oxidized MWCNTs. Strengthening mechanisms were analyzed by SEM images of fracture surfaces and in-situ imaging by digital image correlation (DIC).

Keywords: carbon nanotubes (CNTs); mechanical properties; nanocomposite; vacuum casting.

MeSH terms

  • Epoxy Resins / chemistry*
  • Materials Testing
  • Mechanical Phenomena*
  • Nanocomposites / chemistry*
  • Nanocomposites / ultrastructure
  • Nanotubes, Carbon / chemistry*
  • Nanotubes, Carbon / ultrastructure
  • Porosity
  • Tensile Strength
  • Vacuum*
  • Viscosity

Substances

  • Epoxy Resins
  • Nanotubes, Carbon