Detection of melamine in milk powder using MCT-based short-wave infrared hyperspectral imaging system

Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2018 Jun;35(6):1027-1037. doi: 10.1080/19440049.2018.1469050. Epub 2018 Jun 5.

Abstract

Extensive research has been conducted on non-destructive and rapid detection of melamine in powdered foods in the last decade. While Raman and near-infrared hyperspectral imaging techniques have been successful in terms of non-destructive and rapid measurement, they have limitations with respect to measurement time and detection capability, respectively. Therefore, the objective of this study was to develop a mercury cadmium telluride (MCT)-based short-wave infrared (SWIR) hyperspectral imaging system and algorithm to detect melamine quantitatively in milk powder. The SWIR hyperspectral imaging system consisted of a custom-designed illumination system, a SWIR hyperspectral camera, a data acquisition module and a sample transfer table. SWIR hyperspectral images were obtained for melamine-milk samples with different melamine concentrations, pure melamine and pure milk powder. Analysis of variance and the partial least squares regression method over the 1000-2500 nm wavelength region were used to develop an optimal model for detection. The results showed that a melamine concentration as low as 50 ppm in melamine-milk powder samples could be detected. Thus, the MCT-based SWIR hyperspectral imaging system has the potential for quantitative and qualitative detection of adulterants in powder samples.

Keywords: ANOVA; MCT-based hyperspectral imaging system; food safety; image processing; melamine; partial lease square regression.

MeSH terms

  • Algorithms
  • Animals
  • Cadmium Compounds / chemistry*
  • Food Contamination / analysis*
  • Mercury Compounds / chemistry*
  • Milk / chemistry*
  • Powders / analysis*
  • Spectroscopy, Near-Infrared / instrumentation
  • Spectrum Analysis, Raman / instrumentation
  • Triazines / analysis*

Substances

  • Cadmium Compounds
  • Mercury Compounds
  • Powders
  • Triazines
  • mercury cadmium telluride
  • melamine