Ultraclean pure shift NMR

Chem Commun (Camb). 2017 Sep 12;53(73):10188-10191. doi: 10.1039/c7cc04423b.

Abstract

"Pure shift" methods can greatly improve the resolution of proton NMR spectra. However, current pure shift spectra show small periodic artefacts that prevent their use for studying dilute mixture components. A new technique, compatible with all current pure shift methods, is presented that suppresses such sidebands to arbitrary order, allowing ultraclean spectra to be obtained.