Influence of Light Irradiation Through Zirconia on the Degree of Conversion of Composite Cements

J Adhes Dent. 2016;18(2):161-71. doi: 10.3290/j.jad.a35842.

Abstract

Purpose: To assess the light irradiance (LI) delivered by two light-curing units and to measure the degree of conversion (DC) of three composite cements and one flowable composite when cured through zirconia or ceramic-veneered zirconia plates with different thicknesses.

Materials and methods: Three dual-curing composite cements (Clearfil Esthetic Cement, Panavia F2.0, G-CEM LinkAce) and one light-curing flowable composite (G-aenial Universal Flo) were investigated. Nine different kinds of zirconia plates were prepared from three zirconia grades (YSZ: Aadva and KATANA; Ce-TZP/Al2O3: NANOZR) in three different thicknesses (0.5- and 1.5-mm-thick zirconia, and 0.5-mm-thick zirconia veneered with a 1.0-mm-thick veneering ceramic). Portions of the mixed composite cements and the flowable composite were placed on a light spectrometer to measure LI while being light cured through the zirconia plates for 40 s using two light-curing units (n = 5). After light curing, micro-Raman spectra of the composite films were acquired to determine DC at 5 and 10 min, 1 and 24 h, and at 1 week.

Results: The zirconia grade and the thickness of the zirconia/veneered zirconia plates significantly decreased LI. Increased LI did not increase DC. Only the Ce-TZP/Al2O3 (NANOZR) zirconia was too opaque to allow sufficient light transmission and resulted in significantly lower DC.

Conclusion: Although zirconia-based restorations attenuate the LI of light-curing units, the composite cements and the flowable composite could be light cured through the YSZ zirconia. LI is too low through Ce-TZP/Al2O3 zirconia, necessitating the use of self-/dual-curing composite cements.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aluminum Oxide / chemistry
  • Ceramics / chemistry
  • Ceramics / radiation effects
  • Cerium / chemistry
  • Composite Resins / chemistry
  • Composite Resins / radiation effects*
  • Curing Lights, Dental / classification
  • Dental Materials / chemistry
  • Dental Materials / radiation effects*
  • Dental Veneers
  • Humans
  • Light*
  • Light-Curing of Dental Adhesives / instrumentation
  • Materials Testing
  • Methacrylates / chemistry
  • Microspectrophotometry
  • Polyethylene Glycols / chemistry
  • Polymerization
  • Polymethacrylic Acids / chemistry
  • Polyurethanes / chemistry
  • Radiation Dosage
  • Resin Cements / chemistry
  • Resin Cements / radiation effects*
  • Scattering, Radiation
  • Spectrum Analysis, Raman
  • Surface Properties
  • Yttrium / chemistry
  • Zirconium / chemistry*

Substances

  • Ce-TZP-Al2O3
  • Composite Resins
  • Dental Materials
  • G-Cem resin cement
  • Methacrylates
  • Panavia-Fluoro
  • Polymethacrylic Acids
  • Polyurethanes
  • Resin Cements
  • clearfil esthetic cement
  • yttria stabilized tetragonal zirconia
  • urethane dimethacrylate luting resin
  • triethylene glycol dimethacrylate
  • Cerium
  • Polyethylene Glycols
  • Yttrium
  • Zirconium
  • Aluminum Oxide
  • zirconium oxide