Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2

J Appl Crystallogr. 2015 Nov 19;48(Pt 6):1849-1859. doi: 10.1107/S1600576715019019. eCollection 2015 Dec 1.

Abstract

Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended Q-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc chopper with a variable opening slit window and time-of-flight (TOF) data acquisition option. The chopper used in concert with a dedicated high-intensity velocity selector enables the tuning at will of the wavelength resolution Δλ/λ within a broad range, from 20% (standard) down to 2%, in a convenient and safe manner following pre-planned or spontaneous decisions during the experiment. The new working mode is described in detail, and its efficiency is demonstrated on several standard samples with known properties and on a completely new crystallizable copolymer system, which were investigated using both the conventional (static) and TOF modes.

Keywords: small-angle neutron scattering (SANS); time of flight; wavelength spread.