Sealed rotors for in situ high temperature high pressure MAS NMR

Chem Commun (Camb). 2015 Sep 11;51(70):13458-61. doi: 10.1039/c5cc03910j.

Abstract

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Chemistry Techniques, Analytical / instrumentation*
  • Hot Temperature*
  • Magnetic Resonance Spectroscopy / instrumentation*
  • Pressure*
  • Zirconium / chemistry

Substances

  • Zirconium
  • zirconium oxide